Chromatographic spectra retention of volatile components in the equilibrium vapor phase of medicinal plants “Eucalyptus viminalise Labill”, “Melissa officinalis L.”, “Sophora Japonical L.”
Vestnik Samarskogo universiteta. Estestvennonaučnaâ seriâ, no. 10 (2014), pp. 153-165 Cet article a éte moissonné depuis la source Math-Net.Ru

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Gas chromatographic investigation of headspace of starting materials of herbal origin of Melissa (Melissa officinalis L.), manna gum (Eucalyptus viminalise Labill) and Chinese scholar tree (Sophora Japonical L.) is carried out. For light constituents retention indices $I_i^T$ on capillary column with polydimethylsiloxane stationary phase in the mode of linear programming of temperature and relative areas of peaks $A_{i,\text{отн}} $ are determined. It is established that gas chromatographic spectrum (complex of values $I_i^T$ and $A_{i,\text{отн}}$) of light constituents of headspace has a specific character and may serve as a characteristics of authenticity of starting materials of herbal origin.
Keywords: gas chromatography, Chinese scholar tree, light constituents, chromatographic spectrum.
Mots-clés : Melissa, manna gum, retention indices
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     title = {Chromatographic spectra retention of volatile components in the equilibrium vapor phase of medicinal plants {{\textquotedblleft}Eucalyptus} viminalise {Labill{\textquotedblright},} {{\textquotedblleft}Melissa} officinalis {L.{\textquotedblright},} {{\textquotedblleft}Sophora} {Japonical} {L.{\textquotedblright}}},
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L. A. Onuchak; Yu. I. Arutyunov; E. A. Maskaeva; N. V. Ermakova; A. V. Kurkina. Chromatographic spectra retention of volatile components in the equilibrium vapor phase of medicinal plants “Eucalyptus viminalise Labill”, “Melissa officinalis L.”, “Sophora Japonical L.”. Vestnik Samarskogo universiteta. Estestvennonaučnaâ seriâ, no. 10 (2014), pp. 153-165. http://geodesic.mathdoc.fr/item/VSGU_2014_10_a15/

[1] Onuchak L. A. et al., “Gas chromatographic characteristics of light constituents in fruits and medications of Saint-Mary-thistle”, Journal of Analytical Chemistry, 67:6 (2012), 619–624 (in Russian)

[2] Arutyunov Yu. I., Onuchak L. A., Kurkin V. A. et al., Method of estimate of authenticity of starting materials of herbal origin and mechanism for its realization, Patent no. 2452944 RF; 10.06.2012. Bulletin no. 16, SamSU (in Russian)

[3] Kolb B., Gas chromatography with illustrative materials, Transl. from German by S. Yu. Kudryashov, 2$^{nd}$ ed., revised and enlarged, ed. L. A. Onuchak, Samarskii un-t, Samara, 2007, 247 pp. (in Russian)

[4] Drugov Yu. S., Zenkevich I. G., Rodin A. A., Gas chromatographic identification of air pollution, water pollution, soil pollution and biological media pollution: Practical guidance, 2$^{nd}$ ed., revised and enlarged, Binom. Laboratoriia znanii, M., 2005, 12–14 (in Russian)

[5] van den Dool H., Kratz P. D., “A generalization of the retention index system including liner temperature programmed gas-liquid partition choromatography”, J. of Choromatography, 11:4 (1963), 463–471

[6] Kurkin V. A., Pharmacognosy, 2$^{nd}$ ed., revised and enlarged, OOO “Ofort”, GOU VPO “SamGMU Roszdrava”, Samara, 2007, 1239 pp. (in Russian)

[7] Zuzuk B. M., “Melissa (Melissa officinalis L.): analytical review”, Pharmacist, 2002, no. 1, 36–39 (in Russian)

[8] Popova N. V., “Analysis of essential oil of Melissa”, Pharmacom, 2009, no. 4, 37–40 (in Russian)

[9] General Assay, State Pharmacopoeia of USSR, 1, Issue 11, enlarged edition, Meditsina, M., 1987, 336 pp. (in Russian)

[10] Efremov A. A., Slashchin D. G., Sazonova T. G., Kachin S. V., “Essential oil composition of leaves and stems of Melissa according to the data from chromatography-mass spectrometry”, Analitika Sibiri i Dal'nego Vostoka, Materialy VIII nauchnoi konferentsii (2008), TPU, Tomsk, 2008, 185 (in Russian)

[11] Razhivin R. V., Reteshniak V. Yu. et al., “Application of -mass spectrometry for the study of compositional analysis of pharmacopoeil types of starting materials of herbal origin”, Vestnik of MSU. Ser. 2, 50:1 (2009), 67–70 (in Russian)

[12] Razhivin R. V., Reteshniak V. Yu. et al., “Possibility of application of specific markers of certain types of starting materials of herbal origin at analysis of multicomponent combination herbal medicinal products and herbal medicinal products”, Vestnik of MSU. Ser. 2, 50:2 (2009), 129–132 (in Russian)

[13] E. N. Barata et al., “Identification of host and nonhost semichemicals of eucalyptus woodborer Phoracantha semipunctota by gas chromatography-electroantennography”, J. Chemical of Ecology, 26:8 (2000), 1877–1895 | DOI

[14] Kuz'menko A. N., “Standardization of combination herbal medicinal product by means of gas-liquid chromatography method”, Vestnik of MSU. Ser. 2, 50:4 (2009), 278–281 (in Russian)

[15] Velikorodov A. V., Shevtsova I. A., Fedorovich V. V., “Study of chemical structure of fruits and inflorescences of Chinese scholar tree, introduced in the Astrakhan region”, Experimental chemistry, 2010, no. 2(31), 164–169 (in Russian)

[16] Olennikov D. N., “Fatty acid from seed sophora flavescens and Styphnolobilium japonicum”, Chemistry of Natural Compounds, 45:2 (2009), 225–226 | DOI

[17] Components of essential oils with retention indices on two phases (SE-30 and Carbowax 20M) (in Russian) (accessed July 2012)

[18] NIST Chemistry WebBook, (accessed July 2012) http://webbook.nist.gov/chemistry/

[19] Pavlova L. V., Platonov I. A., Novikova N. V., Nikitcheno N. V., “Chromatography-mass spectrometrical analysis of manna gum (Eucalypti viminalis Labill) with the use of different methods of sample processing”, Analytics and Control, 17:3 (2009), 304–313 (in Russian)