Synthesis of strontium fluoride nanoparticles in a microreactor with intensely swirling flows
Nanosistemy: fizika, himiâ, matematika, Tome 15 (2024) no. 1, pp. 115-121
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The technique of micromixing was used for synthesis of SrF$_2$ nanopowders in a microreactor with intensely swirling flows. The chemical reaction between aqueous solutions of strontium nitrate ($C$(Sr(NO$_3$)$_2$) = 0.15 – 0.45 M) and potassium fluoride ($C$(KF) = 0.3 – 0.9 M) was realized in a microreactor with intensely swirling flows with reagent consumption 1.5 – 3.5 L/min. Colloidal solutions were obtained, during the settling of which SrF$_2$ powders were isolated without crystallographic faceting. An increase in the rate of reagent flow has negligible effect on the size of coherent scattering regions $D$, while an increase in the concentration of solutions leads to an increase in $D$ from $\sim$ 20 to $\sim$30 nm.
Keywords:
strontium fluoride, precipitation, chemical reaction, micromixing.
@article{NANO_2024_15_1_a12,
author = {Rufat Sh. Abiev and Andrey V. Zdravkov and Yuliya S. Kudryashova and Alexander A. Alexandrov and Sergey V. Kuznetsov and Pavel P. Fedorov},
title = {Synthesis of strontium fluoride nanoparticles in a microreactor with intensely swirling flows},
journal = {Nanosistemy: fizika, himi\^a, matematika},
pages = {115--121},
publisher = {mathdoc},
volume = {15},
number = {1},
year = {2024},
language = {en},
url = {http://geodesic.mathdoc.fr/item/NANO_2024_15_1_a12/}
}
TY - JOUR AU - Rufat Sh. Abiev AU - Andrey V. Zdravkov AU - Yuliya S. Kudryashova AU - Alexander A. Alexandrov AU - Sergey V. Kuznetsov AU - Pavel P. Fedorov TI - Synthesis of strontium fluoride nanoparticles in a microreactor with intensely swirling flows JO - Nanosistemy: fizika, himiâ, matematika PY - 2024 SP - 115 EP - 121 VL - 15 IS - 1 PB - mathdoc UR - http://geodesic.mathdoc.fr/item/NANO_2024_15_1_a12/ LA - en ID - NANO_2024_15_1_a12 ER -
%0 Journal Article %A Rufat Sh. Abiev %A Andrey V. Zdravkov %A Yuliya S. Kudryashova %A Alexander A. Alexandrov %A Sergey V. Kuznetsov %A Pavel P. Fedorov %T Synthesis of strontium fluoride nanoparticles in a microreactor with intensely swirling flows %J Nanosistemy: fizika, himiâ, matematika %D 2024 %P 115-121 %V 15 %N 1 %I mathdoc %U http://geodesic.mathdoc.fr/item/NANO_2024_15_1_a12/ %G en %F NANO_2024_15_1_a12
Rufat Sh. Abiev; Andrey V. Zdravkov; Yuliya S. Kudryashova; Alexander A. Alexandrov; Sergey V. Kuznetsov; Pavel P. Fedorov. Synthesis of strontium fluoride nanoparticles in a microreactor with intensely swirling flows. Nanosistemy: fizika, himiâ, matematika, Tome 15 (2024) no. 1, pp. 115-121. http://geodesic.mathdoc.fr/item/NANO_2024_15_1_a12/