Peculiarities of LaFeO$_3$ nanocrystals formation via glycine-nitrate combustion
Nanosistemy: fizika, himiâ, matematika, Tome 8 (2017) no. 5, pp. 647-653
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Varying glycine to nitrate ratio in the initial solution the powders based on nanocrystalline LaFeO$_3$ were synthesized by solution combustion synthesis. The powders were studied by X-ray diffractometry, scanning electron microscopy, adsorption analysis and helium pycnometry. The average crystallite size of the synthesized LaFeO$_3$ nanocrystals ranged from 18 $\pm$ 2 to 85 $\pm$ 9 nm, and the specific surface area of the nanopowders based on them ranged from 8 to 33 m2/g. Based on the results, the influence of redox composition of the reaction solution on the nature of the combustion processes, as well as the composition, structure and properties of LaFeO$_3$ nanocrystals were analyzed. Here, it was shown, that the nanopowders have specific microstructure in terms of monocrystalline nanoscale layers of lanthanum orthoferrite, therefore it is allowed to consider them as a promising base for catalytically and magnetically functional materials.
Keywords:
lanthanum orthoferrite, nanocrystals, formation mechanism, XRD
Mots-clés : glycine-nitrate combustion, SEM.
Mots-clés : glycine-nitrate combustion, SEM.
@article{NANO_2017_8_5_a14,
author = {A. Bachina and V. A. Ivanov and V. I. Popkov},
title = {Peculiarities of {LaFeO}$_3$ nanocrystals formation via glycine-nitrate combustion},
journal = {Nanosistemy: fizika, himi\^a, matematika},
pages = {647--653},
year = {2017},
volume = {8},
number = {5},
language = {en},
url = {http://geodesic.mathdoc.fr/item/NANO_2017_8_5_a14/}
}
TY - JOUR AU - A. Bachina AU - V. A. Ivanov AU - V. I. Popkov TI - Peculiarities of LaFeO$_3$ nanocrystals formation via glycine-nitrate combustion JO - Nanosistemy: fizika, himiâ, matematika PY - 2017 SP - 647 EP - 653 VL - 8 IS - 5 UR - http://geodesic.mathdoc.fr/item/NANO_2017_8_5_a14/ LA - en ID - NANO_2017_8_5_a14 ER -
%0 Journal Article %A A. Bachina %A V. A. Ivanov %A V. I. Popkov %T Peculiarities of LaFeO$_3$ nanocrystals formation via glycine-nitrate combustion %J Nanosistemy: fizika, himiâ, matematika %D 2017 %P 647-653 %V 8 %N 5 %U http://geodesic.mathdoc.fr/item/NANO_2017_8_5_a14/ %G en %F NANO_2017_8_5_a14
A. Bachina; V. A. Ivanov; V. I. Popkov. Peculiarities of LaFeO$_3$ nanocrystals formation via glycine-nitrate combustion. Nanosistemy: fizika, himiâ, matematika, Tome 8 (2017) no. 5, pp. 647-653. http://geodesic.mathdoc.fr/item/NANO_2017_8_5_a14/