X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles
Nanosistemy: fizika, himiâ, matematika, Tome 4 (2013) no. 2, pp. 196-205.

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In the present experimental study, the precipitation of basic yttrium nitrate from aqueous solutions allowed the optimization of conditions for the preparation of loosely aggregated Y$_{2}$(OH)$_{5}$NO$_{3}$ $\cdot$ 1.5H$_{2}$O, the thermal decomposition of which, under controlled annealing, permitted the synthesis of yttria nanoparticles with desirable microstructure. The latter material can be widely used to manufacture yttria optical ceramics. Y$_{2}$(OH)$_{5}$NO$_{3}$ $\cdot$ 1.5H$_{2}$O thermolysis occurs via the formation of a metastable hexagonal Y$_{2}$O$_{3}$ based phase (a = 8.04, c = 12.37 $\mathring{\mathrm{A}}$).
Keywords: yttrium oxide, optical ceramics, X-ray diffraction phase analysis.
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     author = {R. P. Ermakov and V. V. Voronov and P. P. Fedorov},
     title = {X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles},
     journal = {Nanosistemy: fizika, himi\^a, matematika},
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     publisher = {mathdoc},
     volume = {4},
     number = {2},
     year = {2013},
     language = {en},
     url = {http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/}
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R. P. Ermakov; V. V. Voronov; P. P. Fedorov. X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles. Nanosistemy: fizika, himiâ, matematika, Tome 4 (2013) no. 2, pp. 196-205. http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/