X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles
Nanosistemy: fizika, himiâ, matematika, Tome 4 (2013) no. 2, pp. 196-205
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In the present experimental study, the precipitation of basic yttrium nitrate from aqueous solutions allowed the optimization of conditions for the preparation of loosely aggregated Y$_{2}$(OH)$_{5}$NO$_{3}$ $\cdot$ 1.5H$_{2}$O, the thermal decomposition of which, under controlled annealing, permitted the synthesis of yttria nanoparticles with desirable microstructure. The latter material can be widely used to manufacture yttria optical ceramics. Y$_{2}$(OH)$_{5}$NO$_{3}$ $\cdot$ 1.5H$_{2}$O thermolysis occurs via the formation of a metastable hexagonal Y$_{2}$O$_{3}$ based phase (a = 8.04, c = 12.37 $\mathring{\mathrm{A}}$).
Keywords:
yttrium oxide, optical ceramics, X-ray diffraction phase analysis.
@article{NANO_2013_4_2_a4,
author = {R. P. Ermakov and V. V. Voronov and P. P. Fedorov},
title = {X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles},
journal = {Nanosistemy: fizika, himi\^a, matematika},
pages = {196--205},
publisher = {mathdoc},
volume = {4},
number = {2},
year = {2013},
language = {en},
url = {http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/}
}
TY - JOUR AU - R. P. Ermakov AU - V. V. Voronov AU - P. P. Fedorov TI - X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles JO - Nanosistemy: fizika, himiâ, matematika PY - 2013 SP - 196 EP - 205 VL - 4 IS - 2 PB - mathdoc UR - http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/ LA - en ID - NANO_2013_4_2_a4 ER -
%0 Journal Article %A R. P. Ermakov %A V. V. Voronov %A P. P. Fedorov %T X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles %J Nanosistemy: fizika, himiâ, matematika %D 2013 %P 196-205 %V 4 %N 2 %I mathdoc %U http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/ %G en %F NANO_2013_4_2_a4
R. P. Ermakov; V. V. Voronov; P. P. Fedorov. X-ray diffraction study of the phase and morphology changes in yttrium compound nanoparticles. Nanosistemy: fizika, himiâ, matematika, Tome 4 (2013) no. 2, pp. 196-205. http://geodesic.mathdoc.fr/item/NANO_2013_4_2_a4/