Size, morphology and structure of the particles of zirconia nanopowder obtained under hydrothermal conditions
Nanosistemy: fizika, himiâ, matematika, Tome 1 (2010) no. 1, pp. 26-36
Cet article a éte moissonné depuis la source Math-Net.Ru
The morphological and dimensional parameters of the nanoparticles ZrO$_2$, synthesized under hydrothermal conditions are determinate by transmission electron microscopy, small-angle and wide angle X-ray diffraction, dynamic light scattering, adsorption and desorption of gases on the surface. It is shown that only a joint analysis of the results of several methods allows obtaining reliable information about these parameters of the nanoparticles. On the basis of the study obtained under hydrothermal conditions ZrO$_2$ nanoparticles are characterized by an oval (nearly round) shape, narrow particle size distribution and average size of about 12–18 nm.
Mots-clés :
nanoparticles
Keywords: nanopowder, zirconium oxide, hydrothermal synthesis, structure of nanocrystal, form and size nanoparticles, electron microscopy, X-ray scattering, dynamic light scattering.
Keywords: nanopowder, zirconium oxide, hydrothermal synthesis, structure of nanocrystal, form and size nanoparticles, electron microscopy, X-ray scattering, dynamic light scattering.
@article{NANO_2010_1_1_a1,
author = {O. V. Almjasheva and B. A. Fedorov and A. V. Smirnov and V. V. Gusarov},
title = {Size, morphology and structure of the particles of zirconia nanopowder obtained under hydrothermal conditions},
journal = {Nanosistemy: fizika, himi\^a, matematika},
pages = {26--36},
year = {2010},
volume = {1},
number = {1},
language = {ru},
url = {http://geodesic.mathdoc.fr/item/NANO_2010_1_1_a1/}
}
TY - JOUR AU - O. V. Almjasheva AU - B. A. Fedorov AU - A. V. Smirnov AU - V. V. Gusarov TI - Size, morphology and structure of the particles of zirconia nanopowder obtained under hydrothermal conditions JO - Nanosistemy: fizika, himiâ, matematika PY - 2010 SP - 26 EP - 36 VL - 1 IS - 1 UR - http://geodesic.mathdoc.fr/item/NANO_2010_1_1_a1/ LA - ru ID - NANO_2010_1_1_a1 ER -
%0 Journal Article %A O. V. Almjasheva %A B. A. Fedorov %A A. V. Smirnov %A V. V. Gusarov %T Size, morphology and structure of the particles of zirconia nanopowder obtained under hydrothermal conditions %J Nanosistemy: fizika, himiâ, matematika %D 2010 %P 26-36 %V 1 %N 1 %U http://geodesic.mathdoc.fr/item/NANO_2010_1_1_a1/ %G ru %F NANO_2010_1_1_a1
O. V. Almjasheva; B. A. Fedorov; A. V. Smirnov; V. V. Gusarov. Size, morphology and structure of the particles of zirconia nanopowder obtained under hydrothermal conditions. Nanosistemy: fizika, himiâ, matematika, Tome 1 (2010) no. 1, pp. 26-36. http://geodesic.mathdoc.fr/item/NANO_2010_1_1_a1/